Selective separation of indium from zinc, lead, gallium and many other elements by cation-exchange chromatography in hydrohalic acid-acetone medium.
Identifieur interne : 007485 ( Main/Exploration ); précédent : 007484; suivant : 007486Selective separation of indium from zinc, lead, gallium and many other elements by cation-exchange chromatography in hydrohalic acid-acetone medium.
Auteurs : RBID : pubmed:18961581Abstract
Indium can be separated from Zn, Pb(II), Ga, Ca, Be, Mg, Ti(IV), Mn(II), Fe(III), Al, U(VI), Na, Ni(II) and Co(II) by selective elution with 0.50M hydrochloric acid in 30% aqueous acetone from a column of AG50W-X8 cation-exchange resin, all the other elements being retained by the column. Lithium is included in the elements retained by the column when 0.35M hydrochloric acid in 45% aqueous acetone is used for eluting indium, but the elution of indium is slightly retarded. Ba, Sr, Zr, Hf, Th, Sc, Y, La and the lanthanides, Rb and Cs should also be retained according to their distribution coefficients. Cd, Bi(III), Au(III), Pt(IV), Pd(II), Rh(III), Mo(VI) and W(VI) can be eluted with 0.20M hydrobromic acid in 50% aqueous acetone before the elution of indium, and Ir(III), Ir(IV), As(III), As(V), Se(IV), Tl(III), Hg(II), Ge(IV), Sb(III) and Sb(V), though not investigated in detail, should accompany these elements. Relevant distribution coefficients and elution curves and results for analyses of synthetic mixtures of indium with other elements are presented.
PubMed: 18961581
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Selective separation of indium from zinc, lead, gallium and many other elements by cation-exchange chromatography in hydrohalic acid-acetone medium.</title><author><name sortKey="Strelow, F E" uniqKey="Strelow F">F E Strelow</name><affiliation wicri:level="1"><nlm:affiliation>National Chemical Research Laboratory, P.O. Box 395, Pretoria, 0001, South Africa.</nlm:affiliation><country xml:lang="fr">Afrique du Sud</country><wicri:regionArea>National Chemical Research Laboratory, P.O. Box 395, Pretoria, 0001</wicri:regionArea></affiliation></author><author><name sortKey="Wienert, C H" uniqKey="Wienert C">C H Wienert</name></author><author><name sortKey="Van Der Walt, T N" uniqKey="Van Der Walt T">T N van der Walt</name></author></titleStmt><publicationStmt><date when="1974">1974</date><idno type="RBID">pubmed:18961581</idno><idno type="pmid">18961581</idno><idno type="wicri:Area/Main/Corpus">007A09</idno><idno type="wicri:Area/Main/Curation">007A09</idno><idno type="wicri:Area/Main/Exploration">007485</idno></publicationStmt></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Indium can be separated from Zn, Pb(II), Ga, Ca, Be, Mg, Ti(IV), Mn(II), Fe(III), Al, U(VI), Na, Ni(II) and Co(II) by selective elution with 0.50M hydrochloric acid in 30% aqueous acetone from a column of AG50W-X8 cation-exchange resin, all the other elements being retained by the column. Lithium is included in the elements retained by the column when 0.35M hydrochloric acid in 45% aqueous acetone is used for eluting indium, but the elution of indium is slightly retarded. Ba, Sr, Zr, Hf, Th, Sc, Y, La and the lanthanides, Rb and Cs should also be retained according to their distribution coefficients. Cd, Bi(III), Au(III), Pt(IV), Pd(II), Rh(III), Mo(VI) and W(VI) can be eluted with 0.20M hydrobromic acid in 50% aqueous acetone before the elution of indium, and Ir(III), Ir(IV), As(III), As(V), Se(IV), Tl(III), Hg(II), Ge(IV), Sb(III) and Sb(V), though not investigated in detail, should accompany these elements. Relevant distribution coefficients and elution curves and results for analyses of synthetic mixtures of indium with other elements are presented.</div></front></TEI><pubmed><MedlineCitation Owner="NLM" Status="PubMed-not-MEDLINE"><PMID Version="1">18961581</PMID><DateCreated><Year>2008</Year><Month>10</Month><Day>30</Day></DateCreated><DateCompleted><Year>2012</Year><Month>10</Month><Day>02</Day></DateCompleted><Article PubModel="Print"><Journal><ISSN IssnType="Print">0039-9140</ISSN><JournalIssue CitedMedium="Print"><Volume>21</Volume><Issue>11</Issue><PubDate><Year>1974</Year><Month>Nov</Month></PubDate></JournalIssue><Title>Talanta</Title><ISOAbbreviation>Talanta</ISOAbbreviation></Journal><ArticleTitle>Selective separation of indium from zinc, lead, gallium and many other elements by cation-exchange chromatography in hydrohalic acid-acetone medium.</ArticleTitle><Pagination><MedlinePgn>1183-91</MedlinePgn></Pagination><Abstract><AbstractText>Indium can be separated from Zn, Pb(II), Ga, Ca, Be, Mg, Ti(IV), Mn(II), Fe(III), Al, U(VI), Na, Ni(II) and Co(II) by selective elution with 0.50M hydrochloric acid in 30% aqueous acetone from a column of AG50W-X8 cation-exchange resin, all the other elements being retained by the column. Lithium is included in the elements retained by the column when 0.35M hydrochloric acid in 45% aqueous acetone is used for eluting indium, but the elution of indium is slightly retarded. Ba, Sr, Zr, Hf, Th, Sc, Y, La and the lanthanides, Rb and Cs should also be retained according to their distribution coefficients. Cd, Bi(III), Au(III), Pt(IV), Pd(II), Rh(III), Mo(VI) and W(VI) can be eluted with 0.20M hydrobromic acid in 50% aqueous acetone before the elution of indium, and Ir(III), Ir(IV), As(III), As(V), Se(IV), Tl(III), Hg(II), Ge(IV), Sb(III) and Sb(V), though not investigated in detail, should accompany these elements. Relevant distribution coefficients and elution curves and results for analyses of synthetic mixtures of indium with other elements are presented.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Strelow</LastName><ForeName>F E</ForeName><Initials>FE</Initials><Affiliation>National Chemical Research Laboratory, P.O. Box 395, Pretoria, 0001, South Africa.</Affiliation></Author><Author ValidYN="Y"><LastName>Wienert</LastName><ForeName>C H</ForeName><Initials>CH</Initials></Author><Author ValidYN="Y"><LastName>van der Walt</LastName><ForeName>T N</ForeName><Initials>TN</Initials></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType>Journal Article</PublicationType></PublicationTypeList></Article><MedlineJournalInfo><Country>England</Country><MedlineTA>Talanta</MedlineTA><NlmUniqueID>2984816R</NlmUniqueID><ISSNLinking>0039-9140</ISSNLinking></MedlineJournalInfo></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>1974</Year><Month>3</Month><Day>5</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>1974</Year><Month>5</Month><Day>2</Day></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>1974</Year><Month>11</Month><Day>1</Day><Hour>0</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>1974</Year><Month>11</Month><Day>1</Day><Hour>0</Hour><Minute>1</Minute></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>1974</Year><Month>11</Month><Day>1</Day><Hour>0</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pii">0039-9140(74)80101-3</ArticleId><ArticleId IdType="pubmed">18961581</ArticleId></ArticleIdList></PubmedData></pubmed></record>Pour manipuler ce document sous Unix (Dilib)
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